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0406U004736,
к.х.н.
27-11-2006
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Cobalt (II), Nickel (II), Copper (II), Zinc and Cadmium (II) Aquaamminediphosphates
Zhylyak Ivan Dmytrovysh,
popup.head Kopilevch Volodymyr Abramovych
popup.opponent Нагорний Павло Григорович
popup.opponent Власова Наталія Миколаївна
Синтезовано та дослідженно властивостей індивідуальних і гетерометальних подвійних та потрійних аквааміно-дифосфатів Co2+, Ni2+, Cu2+, Zn2+ та Cd2+. Вперше синтезовано речовини складу: 2Cо2P2O7·(6?7)NH3·(8?11)H2O; Ni2P2O7·3NH3·(4?6)H2O; Cu2P2O7·3NH3·(2?3)H2O; 2Zn2P2O7·6NH3·(3?4)H2O Cd2P2O7·3NH3·4,5H2O та гетерометальні акваамінодифосфати кобальту-нікелю, кобальту-міді, нікелю-міді, нікелю-цинку, нікелю-кадмію, міді-цинку, міді-кадмію, нікелю-міді-цинку, нікелю-міді-цинку, нікелю-цинку-кадмію. Їхній склад вивчений методами хімічного і функціонального та рентгенофазового аналізу, спектроскопії. Методом термічного аналізу встановлено послідовності термічних перетворень і складено загальні схеми термолізу. Методом повнопрофільного аналізу Рітвельда встановлено структуру та кристалохімічні характеристики для вперше одержаних безводних дифосфатів.
2006-11-27
2020-04-04
Updated: 2025-12-07
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